NT CAT PC-8 CAS No.:98-94-2 Synthesis method and application Brief introduction. Chemical Chinese name: N,N-dimethylcyclohexylamine Chemical English name: N,N-dimethylcyclohexylamine; dimethyl aminocy clohexane Chemical Alias: Dimethyl aminocyclohexane CAS No.: 98-94-2 EC No.: 202-715-5 Molecular formula: C8H17N Synthesis method. N,N-dimethylaniline catalytic chlorination method In 1904, Sabatier et al. carried out the gas-phase hydrogenation of N,N a dimethylamine at a temperature of 160-180°C and at atmospheric pressure to produce DMCHA. Phenol method This method uses Pd or Rh as the catalyst, and phenol dimethylamine and hydrogen as raw materials. For example, when Pd is the catalyst, the catalyst dosage is 0.2~0.5, and the process conditions are 60~150℃, hydrogen pressure 0.15~0.48MPa, reaction time 6h, and the yield is between 70~80%. The raw material is available, and the reaction conditions are mild, but the catalyst is made of precious metals, and the yield is low. Cyclohexylamine method The process also uses formaldehyde and formic acid to react with cyclohexylamine, or uses oxides of Bi, Sb, Mg, A1, Lu, etc. as catalysts to react cyclohexylamine with methanol to methylate cyclohexylamine to produce DMCHA. the disadvantage of this method is the low selectivity of the former reaction, and the yield of the later methylation is not high. Cyclohexanone method Among the methods for the synthesis of DMCHA, the reductive amination method using cyclohexanone as raw material has more advantages: high conversion, yield and selectivity. The processes using Pd/C catalyst or Cu-A1 catalyst have their own characteristics and are currently under development in China. Uses. [Use I] Mainly used as polyurethane hard foam catalyst [Use II] N,N-dimethylcyclohexylamine can be used in a wide range of rigid foams. N,N-Dimethylcyclohexylamine is also suitable for the manufacture of rigid foam furniture frames and decorative parts. It can be used as the main catalyst alone in rigid foam products without the addition of organotin, or it can be supplemented with JD series catalysts according to the process and product requirements. It is also used as intermediate of rubber accelerator and synthetic fiber. Use III】It is used as intermediate of dyestuff, used to make vanillin, azo dyestuff, triphenylmethane dyestuff, also can be used as solvent, stabilizer, analysis reagent, etc.. Also used as catalyst. Storage and transportation. Should be sealed and stored in a dry, cool and ventilated warehouse Package: 200KG/drum 200KG/drum Storage: It is recommended to store in dry and cool area with proper ventilation. Please fasten the lid as soon as possible after original packaging to prevent the mixing of other substances such as moisture and other substances from affecting the product performance. Do not inhale dust and avoid skin and mucous membrane contact. Smoking, eating and drinking are prohibited in the workplace. After work, shower and change clothes. Store contaminated clothes separately and wash them before use. Maintain good hygiene habits. https://www.newtopchem.com/archives/40458

NT CAT PC-5 CAS No.: 3030-47-5 Product Application Brief introduction. Chemical name: N,N,N′,N′,N″-Pentamethyldiethylenetriamine Alias: Pentamethyldiethylenetriamine Abbreviation: PMDETA English name: N,N,N′,N′,N″-pentamethyldiethylenetriamine Molecular formula: C9H23N3 Relative molecular mass 173.3 CAS No. 3030-47-5 Applications. Pentamethyldiethylenetriamine (PMDETA) is a highly active tertiary amine foaming catalyst, PMDETA has a strong foaming effect, which can improve the flow of foam and enhance the quality of products.PMDETA can also be used as a ligand for polyurethane foam catalysts and a ligand for functional polymerization materials. In addition, other applications are exemplified as follows. 1. Preparation of a two-phase amine absorber for capturing CO2. The two-phase amine absorber is a three-component system consisting of diethylenetriamine, pentamethylenetriamine, and water, and the total concentration of diethylenetriamine and pentamethylenetriamine in water is 4~5 mol/L, and the molar ratio of diethylenetriamine to pentamethylenetriamine is 1:4~4:1; these two organic amines alone do not have the ability to split the phase after absorbing CO2 in aqueous solution, but the two-phase amine absorber composed of the three-phase system But the two-phase amine absorber composed of this ternary system has the performance of phase separation, which is a homogeneous solution before absorbing CO2, and is divided into two phases after absorbing CO2 saturation. After saturated absorption, CO2 is enriched in the aqueous phase, and after phase separation, only the solution enriched in the CO2 phase needs to be regenerated thermally, thus greatly reducing the amount of enriched liquid required for regeneration, effectively reducing regeneration energy consumption, and also maintaining efficient CO2 absorption performance, which has a wide range of application prospects. 2. A methanol gasoline power accelerator. The accelerator consists of: isooctanol, aminoacetaldehyde diethyl acetal, 1,5-cyclooctadiene, 2-acetylbenzofuran, propargyl alcohol, n-propanol, zinc naphthenate, dinonyl naphthalene sulfonic acid, dipolyoxyvinyl aliphatic amine, and pentamethyldiethylenetriamine. The preparation method includes: a. Add isooctanol, aminoacetaldehyde diethyl acetal, 1,5-cyclooctadiene, 2-acetylbenzofuran to the reaction kettle and stir the reaction for 40-50 minutes at 60-62°C with closed ultrasonic stirring, b. Mix n-propanol, zinc naphthenate, dinonyl naphthalenesulfonic acid and stir for 15-25 minutes; c. Add propargyl alcohol, the mixture in step b, dipolyoxyvinyl fatty amine, pentamethyl diethylenetriamine, add them to the mixture in step a in turn, stir for 20~25 minutes at 33~35℃, and then cool down to obtain. Quality index. Content: ≥98% Specific gravity: 0.8330-0.8410 Refractive index: 1.4430-1.4450 Storage and transportation. Should be sealed and stored in a dry, cool and ventilated warehouse Packing. 200KG/drum Storage: It is recommended to be stored in dry and cool area with proper ventilation. Please fasten the lid as soon as possible after the original packaging to prevent the mixing of other substances such as water and other substances from affecting the product performance. Do not inhale dust and avoid skin and mucous membrane contact. Smoking, eating and drinking are prohibited in the workplace. After work, shower and change clothes. Store contaminated clothes separately and wash them before use. Maintain good hygiene habits. https://www.newtopchem.com/archives/668

N-methyl-Methylcyclohexylamine CAS 100-60-7 Descriptions： Synonyms： Cyclohexylmethylaminecyclohexyl-methyl-aminemethylcyclohexylamine,[corrosivelabel]Cyclohexylamine,N-methyl-1-MethylcyclohexylamineCyclohexanamine,N-methyl-MethylcyclohexylamineN-Cyclohexylmethylamine CAS No.：100-60-7 Molecular Formula：C7H15N ( Isomeride) Molecular Weight：113.204 EINECS：202-869-3 Category：Pharmaceutical Intermediates Physicochemical properties Density：0.868 Melting point：-8℃ Boiling point：149℃ Refractive index：1.4545-1.4565 Flash point：29℃ Vapor pressure：4.62mmHg at 25°C PSA：12.03000 logP：1.92940 Appearance：transparent and colorless liquid Color： colorless liquid Physical Property：transparent and colorless liquid， Miscible with various organic solvents, slightly soluble in water。Melting point：＆＃8722；9-＆＃8722；7＆＃160；＆＃x00b0；C(lit.) Boiling point：149＆＃160；＆＃x00b0；C(lit.) Density：0.868＆＃160；g/mL＆＃160；at 25＆＃160；＆＃x00b0；C(lit.) Refractive index：n20/D 1.456(lit.) Flash point：85＆＃160；＆＃x00b0；F Water solubility：5.4 g/100 mL (20 ＆＃186；C) transparent and colorless liquid. Miscible with various organic solvents, slightly soluble in water。 transparent and colorless liquid。 Boiling point 147~151℃ Relative density 0.868 Refractive index 1.4456 Flash point 29℃ Solubility Miscible with various organic solvents, slightly soluble in water Solubility：Slightly soluble in water, soluble in benzene, alcohol, etc Application： Used as intermediates in medicine and dyes Pharmaceutical and dye intermediates. Used as an intermediate in the drug bromohexamine hydrochloride Production Method： With cyclohexylamine as raw material prepared. 2. By the reaction of cyclohexanone and methylamine. Soak aluminum sheet in methanol, add high mercury chloride, continue to soak 2h, temperature rise does not exceed 55℃, remove the soaking liquid. Add ethanol to the activated aluminum sheet, drop the mixture of methylamine and cyclohexanone under agitation, heat reflux, and place overnight. Adding 10% sodium hydroxide solution alkalization, extracting with benzene twice, after washing by distillation, benzene recovery that distillation of n-methyl cyclohexylamine. The yield is about 80%. ; Storage and transport information：： It should be sealed and stored in a dry and cool ventilated warehouse Packaging： 200KG/ drum storage: It is recommended to store in dry and cool areas and properly ventilated. After the original packaging, please fasten the packaging cover as soon as possible to prevent moisture and other substances from mixing and affecting the product performance. Do not inhale dust and avoid skin and mucous membrane contact. Smoking, eating and drinking are prohibited in the workplace. After work, shower and change. Store contaminated clothes separately and reuse them after washing. Maintain good hygiene. Contact Us SHANGHAI OHANS CO., LTD. Factory Address ：Jining High-tech Development Zone, Shandong, China Call Center ：021-5161-9971 Headquarters ：Room a2110, building 55, No. 709, Lingshi Road, Zhabei District, Shanghai Email Us ：[email protected] [email protected] More：https://www.ohans.com/n-methyl-methylcyclohexylamine-cas-100-60-7-pdf/